The first results of measuring XAFS spectra in the soft X-ray range at KOSMOS station

13 Jul 2020, 20:30
19m
Poster SR technological application and X-ray apparatus Poster Session

Speakers

Anton Nikolenko (Budker INP SB RAS) Mikhail Syrokvashin (NIIC SB RAS)

Description

XAFS spectra were measured near the K edges of the absorption of phosphorus, sulfur, and L III absorption edges of molybdenum and niobium (2100 - 2700 eV). The measurements were carried out using an upgraded Si (111) dual-crystal monochromator in normal incidence geometry. The monochromator device is described. The main difficulties arising in the course of obtaining spectra are discussed. It is shown that the spectral resolution of the monochromator allows one to obtain XAFS spectra, the quality of which is sufficient to decipher the structure of the sample. The measurement was carried out with a partial funding from the Russian Science Foundation (project No. 18-03-01061).

Primary author

Anton Nikolenko (Budker INP SB RAS)

Co-authors

Anastasiya Fedorenko (NIIC SB RAS) Denis Ivlyushkin (Budker INP SB RAS) Evgeniy Korotaev (Nikolaev Institute of Inorganic Chemistry of the Siberian Branch of the Russian Academy of Sciences) Mikhail Syrokvashin (NIIC SB RAS) Pavel Zavertkin (Budker INP SB RAS)

Presentation Materials