The project of the beam-line "Structure investigation" at synchrotron radiation source SKIF in Novosibirsk

Not scheduled
15m
Conference Hall (Budker INP)

Conference Hall

Budker INP

Lavrentiev av. 11, Novosibirsk 630090 Russia
Poster X-ray structural analysis

Speakers

Prof. Boris Tolochko (Institute of solid state chemistry and mechanochemistry) Mr Oleg Evdokov (Institute of Solid State Chemistry and Mechanochemistry SB RAS)

Description

A new beamline "Structure investigation" will be put into operation in the test mode at the SKIF synchrotron radiation source in 2024. The beamline will have stations: 1) "Precision diffraction / anomalous scattering"; 2) "In situ diffraction"; 3) "Single crystal diffraction"; 4) «USAXS / reflectometry». The stations will supervise accordingly: 1) Institute of Catalysis of the SB RAS; 2) Institute of Solid State Chemistry and Mechanochemistry of the SB RAS; 3) Institute of Inorganic Chemistry of SB RAS; 4) Shubnikov Institute of Crystallography RAS. The beamline will use the radiation from a 300-pole superconducting undulator with a 1.2 T field. At a photon energy of 7 keV, the brightness will be 4*10 ^ 21 phot / (sec mm^2 mrad^2 0.1% BW). The energy range will be from 5 to 50 keV. Required channel element will be beam monitor. The monitor will determine both the intensity of the beam and its position with an accuracy of 1 micron. The read out frequency of monitor will be 100 MHz, which will allow to determine the position of the radiation from each bunch of electrons. A dual monochromator with a fixed output can provide monochromatization from 10^-2 to 10^-4. If necessary, a monochromator can skip a white beam. Focusing mirrors will be used, which will ensure focusing and cutting of high harmonics if necessary. To work in a high energy area, refractive optics will be used. Both focusing and defocusing lens will be used. A fast chopper will be used, for investigating of fast processes, with exposure from a single bunch with continuance near 73 ps. The main detector at the new station will be the coordinate-sensitive detectors DIMEX [1], whose use at the VEPP-3 source and showed great potential possibilities associated with the use of synchrotron radiation for the study of fast processes [2]. Detectors OD-3M [3] and PILATUS will also be used. [1] V.M. Aulchenko, B.P. Tolochko, L.I. Shekhtman, et al. Fast high resolutuion gaseous detectors for diffraction experiments and imaging at synchrotron radiation beam. Nuclear Instr. and Meth. A 623 (2010) 600-602. [2] K.A. Ten, E.R. Pruuel, V.M. Titov. SAXS Measurement and Dynamics of Condensed Carbon Growth at Detonation of Highly Explosive. Fullerenes, Nanotubes, and Carbon Nanostructures. 20: 587-593. 2012. [3] Aulchenko, V.M., Evdokov, O.V., Kutovenko, V.D., Pirogov, B.Ya., Sharafutdinov, M.R., Titov, V.M., Tolochko, B.P., Vasiljev, A.V., Zhogin, I.A., Zhulanov, V.V. One-coordinate X-ray detector OD-3M (2009) Nuclear Instruments and Methods in Physics Research, Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, 603 (1-2), pp. 76-79.

Primary author

Prof. Boris Tolochko (Institute of solid state chemistry and mechanochemistry)

Co-authors

Mr Aleksandr Kosov (Budker INP SB RAS) Dr Alexander Shmakov (Boreskov Institute of Catalysis SD RAS) Dr Konstantin Zolotarev (Budker Institute of Nuclear Physics) Mr Lev Shekhtman (Budker Institute of Nuclear Physics) Mr Marat Sharafutdinov (ISSCM SB RAS, BINP SB RAS) Mr Oleg Evdokov (Institute of Solid State Chemistry and Mechanochemistry SB RAS) Prof. Serg Gromilov (Institute inorganic Chemistry SB RAS) Prof. Victor Asadchikov (FSRC "Crystallography and photonics" RAS) Dr Vitaly Titov (Institute of nuclear physics SB RAS) Mr Vladimir Aulchenko (BINP) Dr Vladimir Zhulanov (Budker INP)

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